HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl acetylenedicarboxylate → HCID 21860267, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl acetylenedicarboxylate | HCID 12980 | — |
| Reactant | 5-amino-1,3-diphenylpyrazole-4-carbonitrile | HCID 2754619 | — |
| Product | HCID 21860267 | HCID 21860267 | — |
Reaction Steps
Using 2.60 g (10 mmol) of 5-amino-1,3-diphenylpyrazole-4-carbonitrile [see J. Org. Chem., 29, 1915 (1964)] and 1.42 g (10 mmol) of dimethyl acetylenedicarboxylate, the entitled product having a melting point of 277° to 279° C. was obtained in the same manner as in Example 2-(2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05801008 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-c274db0a2ffb4a01b4f29da2b7007240 |
| Source note | uspto-grants-1998_09 |