4-Carboxyphenylboronic Acid → HCID 18980090, compound

HRID 2392654Notes

Reaction equation

HRID 2392654 reaction equation
Br[C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH:12]=[N:11][CH:10]=[N:9]2)=[CH:4][C:3]=1[CH3:13].B([C:17]1[CH:25]=[CH:24][C:20]([C:21]([OH:23])=[O:22])=[CH:19][CH:18]=1)(O)O>>[CH3:13][C:3]1[CH:4]=[C:5]([N:8]2[CH:12]=[N:11][CH:10]=[N:9]2)[CH:6]=[CH:7][C:2]=1[C:17]1[CH:25]=[CH:24][C:20]([C:21]([OH:23])=[O:22])=[CH:19][CH:18]=1

Participants

3

Reactant 2

HCID 3121834-Carboxyphenylboronic AcidHCID 189801161-(4-Bromo-3-methylphenyl)-1,2,4-triazole

Product 1

HCID 18980090HCID 18980090, compoundYield 63.9%

Procedure

The title compound (0.15 g) was prepared from 1-(4-bromo-3-methylphenyl)-1,2,4-triazole (D63, 0.2 g) and 4-boronobenzoic acid (0.14 g) as described in Description 15.

Sources & evidence

ORD record
ord-6a7d17549ef44441ab544d0834f6d44b
Source dataset
uspto-grants-1998_09
Patent number
US05801170

Reaction notes

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