2-Chloro-5-nitrophenol → HCID 18980072, compound

HRID 2392658Notes

Reaction equation

HRID 2392658 reaction equation
Br[C:2]1[CH:7]=[CH:6][C:5]([N:8]2[N:12]=[N:11][CH:10]=[N:9]2)=[CH:4][CH:3]=1.B([C:16]1[CH:24]=[CH:23][C:19]([C:20]([OH:22])=[O:21])=[CH:18][CH:17]=1)(O)O.ClC1C=CC([N+]([O-])=O)=CC=1O>>[N:9]1[N:8]([C:5]2[CH:6]=[CH:7][C:2]([C:16]3[CH:24]=[CH:23][C:19]([C:20]([OH:22])=[O:21])=[CH:18][CH:17]=3)=[CH:3][CH:4]=2)[N:12]=[N:11][CH:10]=1

Participants

4

Reactant 3

HCID 692642-Chloro-5-nitrophenolHCID 3121834-Carboxyphenylboronic AcidHCID 5608042-(4-Bromophenyl)-2H-tetrazole

Product 1

HCID 18980072HCID 18980072, compound

Procedure

The title compound was prepared from 2-(4-bromophenyl)tetrazole (D72, 0.2 g) and 4-boronobenzoic acid (0.15 g) as described in Description 15 (0.17 g, 72%).

Sources & evidence

ORD record
ord-0d5f6f6053b741ea8b86db2702cb9059
Source dataset
uspto-grants-1998_09
Patent number
US05801170

Reaction notes

Loading…