HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromoanisole → HCID 18980470, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromoanisole | HCID 16971 | — |
| Reactant | HCID 18980453 | HCID 18980453 | — |
| Product | HCID 18980470 | HCID 18980470 | 47% |
Reaction Steps
The base of compound (27) was reacted with 1-bromo-3-methoxy-benzene corresponding to the conditions described in Example 1. The base obtained was purified with 6:1 ethyl acetate/methanol via a silica gel column and was taken up in 2-butanone. After adding trimethylchlorosilane/water, compound (24) was obtained in a yield of 47% theoretical.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05801201 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-d895e9190ff54e15aa925cd63c8d4f22 |
| Source note | uspto-grants-1998_09 |