HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → HCID 22446842, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | (2-Bromoethyl)cyclopentane | HCID 12711948 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 22446842 | HCID 22446842 | — |
Reaction Steps
17.7 g (100 mmole) (2-bromoethyl)-cyclopentane, 32.5 g (124 mmole) triphenylphosphine and 100 ml toluene were boiled for 56 hours under reflux. The mixture was stirred overnight at room temperature. The crystals formed were filtered off by suction, washed with ether and dried under vacuum. The yield of compound (53) was 35.6 g (82% theoretical).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05801201 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-7c5c10429cce49108737a51283987f1a |
| Source note | uspto-grants-1998_09 |