HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 532511, compound → HCID 18977784, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 532511 | HCID 532511 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18977784 | HCID 18977784 | — |
Reaction Steps
16.9 g (0.042 mol) of 4-benzoxyphenyl 4-methylbenzoate are added to 250 ml of ethanol and hydrogenated at room temperature using Raney nickel under a hydrogen atmosphere at atmospheric pressure. The catalyst is subsequently filtered off with suction and destroyed using ethanol. The filtrate is evaporated, and the product is purified by filtration through silica gel.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05804097 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-334a15d38f8544d5b6457fe54e2ea850 |
| Source note | uspto-grants-1998_09 |