Fumarate → HCID 131720819, compound

HRID 2393272Notes

Reaction equation

[Cl:1][C:2]1[CH:10]=[C:9]2[C:5]([C@H:6]([C:22]3[CH:27]=[CH:26][C:25]([F:28])=[CH:24][CH:23]=3)[CH2:7][C@H:8]2[N:11]2[CH2:20][C:15]3([CH2:19]C[CH2:17][CH2:16]3)[N:14]([CH3:21])[CH2:13][CH2:12]2)=[CH:4][CH:3]=1.C([O-])(=O)/C=C/C([O-])=O>>[ClH:1].[ClH:1].[Cl:1][C:2]1[CH:10]=[C:9]2[C:5]([C@H:6]([C:22]3[CH:23]=[CH:24][C:25]([F:28])=[CH:26][CH:27]=3)[CH2:7][C@H:8]2[N:11]2[CH2:20][C:15]3([CH2:19][CH2:17][CH2:16]3)[N:14]([CH3:21])[CH2:13][CH2:12]2)=[CH:4][CH:3]=1

Participants

Reactant 2

HCID 5460307Fumarate

HCID 70278587HCID 70278587, compound

Product 1

HCID 131720819HCID 131720819, compound

Procedure

(±)-Trans-9-[6-chloro-3-(4-fluorophenyl)-2,3-dihydro- 1H-inden- 1-yl]-6-methyl-6,9-diazaspiro[4.5]decane, fumarate; mp 144°-147° C. Compd. 29.

Sources & evidence

ORD record: ord-14cc0f5ca61d4d95a1eb336c8fa4e85d
Source dataset: uspto-grants-1998_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05807855

Reaction notes

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