HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Nitro-2,3-dihydro-1H-inden-1-amine--hydrogen chloride (1/1) → HCID 23298452, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Nitro-2,3-dihydro-1H-inden-1-amine--hydrogen chloride (1/1) | HCID 23298400 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 23298452 | HCID 23298452 | — |
Reaction Steps
To a solution of 6-nitro-1-aminoindane hydrochloride (1.00 g, 4.66 mmol) in MeOH (100 ml) was added a catalytic amount of 10% Pd/C. The mixture was hydrogenated at 50 psi for 1 hr, filtered through celite, and concentrated to give 6-amino-1-aminoindane hydrochloride which was homogeneous by TLC and used immediately in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05807886 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-6ffb8232c8d04f53b95350857f394d76 |
| Source note | uspto-grants-1998_09 |