Dimesitylboron fluoride → HCID 18787989, compound

HRID 2393676Notes

Reaction equation

[Cl:1][C:2]1[C:7]([CH3:8])=[CH:6][C:5]([CH3:9])=[C:4]([B:10]([C:12]2[C:17]([CH3:18])=[C:16]([Cl:19])[C:15]([CH3:20])=[CH:14][C:13]=2[CH3:21])F)[C:3]=1[CH3:22].[C:23]1([CH3:42])[CH:28]=[C:27]([CH3:29])[CH:26]=[C:25]([CH3:30])[C:24]=1[B:31]([C:33]1[C:38]([CH3:39])=[CH:37][C:36]([CH3:40])=[CH:35][C:34]=1[CH3:41])F>>[Cl:1][C:2]1[C:7]([CH3:8])=[CH:6][C:5]([CH3:9])=[C:4]([B:10]([C:12]2[C:17]([CH3:18])=[C:16]([Cl:19])[C:15]([CH3:20])=[CH:14][C:13]=2[CH3:21])[C:2]2[CH:7]=[CH:6][CH:5]=[C:4]([B:31]([C:33]3[C:38]([CH3:39])=[CH:37][C:36]([CH3:40])=[CH:35][C:34]=3[CH3:41])[C:24]3[C:25]([CH3:30])=[CH:26][C:27]([CH3:29])=[CH:28][C:23]=3[CH3:42])[CH:3]=2)[C:3]=1[CH3:22]

Participants

Reactant 2

HCID 3466040Dimesitylboron fluoride

HCID 18787960HCID 18787960, compound

Product 1

HCID 18787989HCID 18787989, compoundYield 86%

Procedure

The compound is prepared by Method B described above in a yield of 86%, using 1 equivalent of bis(chloromesityl)fluoroborane and 1 equivalent of dimesitylfluoroborane. Physical data are given in Table 1.

Workup

customThe compound is prepared by Method B

Sources & evidence

ORD record: ord-6615ee581be34e038b287de2fe9a771e
Source dataset: uspto-grants-1998_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05807905

Reaction notes

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