HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diphenylphosphoryl azide → 5-[(1R)-1-Azidobutyl]-1,3-benzodioxole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diphenylphosphoryl azide | HCID 123414 | — |
| Reactant | HCID 10375365 | HCID 10375365 | — |
| Reactant | HCID 18977048 | HCID 18977048 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 5-[(1R)-1-Azidobutyl]-1,3-benzodioxole | HCID 10680381 | — |
Reaction Steps
tR : α-propyl-piperonyl alcohol, 5.9 min.; toluene, 7.8 min.; (PhO)2P(O)N3, 9.3 min.; olefin side-product, 10.6 min.; α-propyl-piperonylazide, 11.4 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05808056 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-c60bb8129bd1420183f8f2ba612550c8 |
| Source note | uspto-grants-1998_09 |