HRID2393853

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CC#CC1=CCC(C)(C)c2cc(C#Cc3ccc(C(=O)OCC)cc3)ccc21

HCID18314565

未命名化合物

2 次

结构：CC1(C)CC=C(c2ccccc2)c2ccc(C#Cc3ccc(C(=O)O)cc3)cc21

HCID18314590

未命名化合物

2 次

PRODUCTS

生成物

结构：CC#CC1=CCC(C)(C)c2cc(C#Cc3ccc(C(=O)O)cc3)ccc21

HCID18314573

未命名化合物

PROCEDURE

实验过程

Employing the same general procedure as for the preparation of 4-[(7,8-dihydro-8,8-dimethyl-5-phenylnaphth-2-yl)ethynyl]benzoic acid (Compound 97), 75 mg (0.20 mmol) of ethyl 4-[(7,8-dihydro-8,8-dimethyl-5-(1-propynyl)naphth-2-yl)ethynyl]benzoate (Compound 92) was converted to the title compound (pale yellow solid) using 42 mg (2 ml, 1.0 mmol) of LiOH (0.5M aqueous solution).