Benzene, [1-[(trimethylsilyl)oxy]ethenyl]- → HCID 54681269, compound

Participants

Reaction Steps

The title compound was prepared by Method A using 1-phenyl-1-(trimethylsilyloxy)ethylene (1.95 g, 10.14 mmol) and diethyl ester of [(2,6-dimethylphenyl)thio]propanedioic acid (2.0 g, 6.8 mmol). m.p. 248°-249° C.; 1H NMR (400 MHz, DMSO-d6) δ 2.47 (s, 6H), 6.75 (s, 1H), 7.08 (m, 3H), 7.39 (m, 3H), 7.78 (m, 2H).

Provenance & Evidence