Benzene, [1-[(trimethylsilyl)oxy]ethenyl]- → HCID 54681205, compound

Participants

Reaction Steps

The title compound was prepared by Method A using 1-phenyl-1-(trimethylsilyloxy)ethylene (1.95 g, 10.14 mmol) and diethyl ester of [(2-chlorophenyl)thio]propanedioic acid (1.53 g, 5.07 mmol). m.p. 275°-280° C.; 1H NMR (400 MHz, DMSO-d6) δ 6.78 (s, 1H), 6. 89 (dd, 1H), 7. 08 (tt, 1H), 7. 19 (tt, 1H), 7.42 (dd, 1H), 7.56 (m, 3H), 8.06 (m, 2H).

Provenance & Evidence