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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2394231Generated: October 25, 2026

Benzothiazole → 1-Methyl-4-Prop-1-En-2-Ylcyclohexene

https://huagongshe.com/reaction/2394231

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzothiazoleHCID 7222—
ReactantCarvone, (+-)-HCID 7439—
Reactant2-Cyclopenten-1-one, 3-methyl-2-(2Z)-2-pentenyl-HCID 10261—
ReactantJasmoneHCID 1549018—
Product1-Methyl-4-Prop-1-En-2-YlcyclohexeneHCID 22311—
ProductLimonene oxideHCID 91496—
Product(+)-LimoneneHCID 440917—

Reaction Steps

Benzothiazole, an aromatic sulfonazole, was obtained from Sigma-Aldrich in a 96% formulation, catalog No.1-133-8. Carvone, a 6-carbon ring terpene with ketone on the ring, in particular, (2-methyl-5-(1-methylethyenyl)- 2-cylco-hexene-1 -one, was obtained from Sigma-Aldrich in a 98% formulation, catalog No. 12393-1. Cis-jasmone, a terpene with the chemical name 3- methyl-2-(2-pentenyl)-2-cylco-penten-1-one, was obtained from Sigma-Aldrich in a 90% formulation, catalog No. 277444. Limonene, a terpene, was obtained in a 97% mixture of cis and trans forms of limonene oxide, chemica name 1-methyl-4-(1-methylethenyl) cylcohexene, from Sigma-Aldrich, catalog No. 21832-4. Cinieole, a terpene with the chemical name 1,3,3-trimethyl-2- oxabicyclo-(2.2.2)octane, was obtained from Sigma-Aldrich in a 99% formulation, catalog No. C8060-1. Trans-cinnamaldehye, an aromatic aldehyde with the chemical name 3-phyl-2-propenal was obtained from Sigma-Aldrich in a 99+% formulation, catalog No. 23996-8.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05811372
Source datasetuspto-grants-1998_09
ORD IDord-1f38dd9d599840899663f633079039b5
Source noteuspto-grants-1998_09