HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 54156557, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 18973197 | HCID 18973197 | — |
| Reactant | Ethylorthoformate | HCID 53630039 | — |
| Product | HCID 54156557 | HCID 54156557 | — |
Reaction Steps
305 g (1.24 mol) of ethyl 4,5,5-trichloro-3-oxo-4-pentenecarboxylate are heated with 275 g (1.86 mol) of ethyl orthoformate and 316.0 g of acetic anhydride at 150°-160° C. for three hours. All volatile components are removed initially in vacuo, then under a high vacuum up to 100° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05811433 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-48c5e4592b904c80888ae1ab86e1395a |
| Source note | uspto-grants-1998_09 |