HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosulfonyl isocyanate → HCID 18973106, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosulfonyl isocyanate | HCID 70918 | — |
| Reactant | HCID 18973052 | HCID 18973052 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 18973106 | HCID 18973106 | — |
Reaction Steps
The title compound was prepared from 3-(2-thenoyl)-6-azaoxindole (Example 38) according to the procedure of Example 2C, using 3-(2-thenoyl)-6-azaoxindole (3.09 g, 12.6 mmol), N-chlorosulfonyl isocyanate (1.2 mL, 13.8 mmol) and acetonitrile (60 mL). Reaction time: 31/2 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05811432 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-a9e26d15652342818e698ddb47b8fb36 |
| Source note | uspto-grants-1998_09 |