HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Furancarbonyl chloride → HCID 18973113, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Furancarbonyl chloride | HCID 68242 | — |
| Reactant | HCID 18973025 | HCID 18973025 | — |
| Catalyst | 4-(Dimethylamino)pyridine | HCID 14284 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 18973113 | HCID 18973113 | — |
Reaction Steps
The title compound was prepared from 5-chloro-1-ethyl-7-azaoxindole (Example 53D) according to the procedure of Example 53E, using 5-chloro-1-ethyl-7-azaoxindole (405 mg, 2.06 mmol), 4-dimethylaminopyridine (500 mg, 4.09 mmol), 2-furoyl chloride (0.22 mL, 2.23 mmol) and DMF (10 mL). The solid product obtained following chromatography was recrystallized from hexane. The yield was 110 mg (18%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05811432 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-a2b54ea3fd944c3d8262740f7a884c90 |
| Source note | uspto-grants-1998_09 |