Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2394374Generated: November 1, 2026

2-Furancarbonyl chloride → HCID 18973113, compound

https://huagongshe.com/reaction/2394374

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-Furancarbonyl chlorideHCID 68242—
ReactantHCID 18973025HCID 18973025—
Catalyst4-(Dimethylamino)pyridineHCID 14284—
SolventDimethylformamideHCID 6228—
ProductHCID 18973113HCID 18973113—

Reaction Steps

The title compound was prepared from 5-chloro-1-ethyl-7-azaoxindole (Example 53D) according to the procedure of Example 53E, using 5-chloro-1-ethyl-7-azaoxindole (405 mg, 2.06 mmol), 4-dimethylaminopyridine (500 mg, 4.09 mmol), 2-furoyl chloride (0.22 mL, 2.23 mmol) and DMF (10 mL). The solid product obtained following chromatography was recrystallized from hexane. The yield was 110 mg (18%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05811432
Source datasetuspto-grants-1998_09
ORD IDord-a2b54ea3fd944c3d8262740f7a884c90
Source noteuspto-grants-1998_09