HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N-Dimethyl-1H-imidazole-1-sulfonamide → HCID 178486172, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N-Dimethyl-1H-imidazole-1-sulfonamide | HCID 395751 | — |
| Reactant | Zincchloride | HCID 3007855 | — |
| Reactant | HCID 178418306 | HCID 178418306 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178486172 | HCID 178486172 | — |
Reaction Steps
N-dimethylsulfamoyl-imidaz-2-yl zinc chloride was prepared in situ by lithiation of N-dimethylsulfamoylimidazole (0.97 g, 5.5 mmol) in THF (20 mL) with t-BuLi (1.7M, 6.7 mL), followed by quenching with zinc chloride (1.87 g, 13.75 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05811422 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-537a3f9e44294d5ebb525724eb399c1c |
| Source note | uspto-grants-1998_09 |