HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylimidazole → 1-((6-chloro-1,3-benzodioxol-5-yl)methyl)2-methyl-1H-imidazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylimidazole | HCID 12749 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 6-Chloropiperonyl chloride | HCID 90113 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 1-((6-chloro-1,3-benzodioxol-5-yl)methyl)2-methyl-1H-imidazole | HCID 21224807 | — |
Reaction Steps
The operation is carried out as in Stage 1 of Example 11 starting with 12.3 g of 2-methyl-1H-imidazole, 7.92 g of sodium hydride with 50% oil, 150 ml of N dimethylformamide and 33.8 g of 6-chloropiperonyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05811444 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-b0355b73ad444415877314fc2a7b959b |
| Source note | uspto-grants-1998_09 |