Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Indole-4-carboxaldehyde → 1-[2-(Thien-2-yl)ethyl]indole-4-carbaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Indole-4-carboxaldehyde | HCID 333703 | — |
| 반응물 | 2-(2-Thienyl)ethyl methanesulphonate | HCID 3047723 | — |
| 생성물 | 1-[2-(Thien-2-yl)ethyl]indole-4-carbaldehyde | HCID 18973449 | 39.1% |
반응 단계
The same procedures used in Example 1 were repeated except for using 435 mg of indole-4-carbaldehyde and 680 mg of 2-(thien-2-yl)ethyl methanesulfonate instead of the benzyl bromide used in Example 1 to give 299 mg of 1-[2-(thien-2-yl)ethyl]indole-4-carbaldehyde as an orange-colored oily substance. The yield thereof was found to be 39%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05811439 |
| 출처 데이터셋 | uspto-grants-1998_09 |
| ORD ID | ord-4573cf993a3f4246baa35f49df38e063 |
| 출처 메모 | uspto-grants-1998_09 |