3-Bromocyclohexene → HCID 18973331, compound

HRID 2394423Notes

Reaction equation

HRID 2394423 reaction equation
Br[CH:2]1[CH2:7][CH2:6][CH2:5][CH:4]=[CH:3]1.[NH:8]1[C:16]2[CH:15]=[CH:14][CH:13]=[C:12]([CH:17]=[O:18])[C:11]=2[CH:10]=[CH:9]1>>[CH:2]1([N:8]2[C:16]3[CH:15]=[CH:14][CH:13]=[C:12]([CH:17]=[O:18])[C:11]=3[CH:10]=[CH:9]2)[CH2:7][CH2:6][CH2:5][CH:4]=[CH:3]1

Participants

3

Reactant 2

HCID 1370573-BromocyclohexeneHCID 333703Indole-4-carboxaldehyde

Product 1

HCID 18973331HCID 18973331, compoundYield 17.9%

Procedure

The same procedures used in Example 1 were repeated except for using 2.44 g of 3-bromocyclohexene and 2.00 g of indole-4-carbaldehyde as a starting material to give 556 mg of 1-(2-cyclohexenyl)indole-4-carbaldehyde as a yellow-colored oily substance. The yield thereof was found to be 18%.

Sources & evidence

ORD record
ord-902c050ced7741169b9a3213eedf9c8b
Source dataset
uspto-grants-1998_09
Patent number
US05811439

Reaction notes

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