Indole-4-carboxaldehyde → HCID 18973322, compound
Reaction equation
[NH:1]1[C:9]2[CH:8]=[CH:7][CH:6]=[C:5]([CH:10]=[O:11])[C:4]=2[CH:3]=[CH:2]1.CS(O[CH:17]([CH3:24])[CH2:18][CH2:19][CH:20]=[C:21]([CH3:23])[CH3:22])(=O)=O>>[CH3:22][C:21](=[CH:20][CH2:19][CH2:18][CH:17]([N:1]1[C:9]2[CH:8]=[CH:7][CH:6]=[C:5]([CH:10]=[O:11])[C:4]=2[CH:3]=[CH:2]1)[CH3:24])[CH3:23]Participants
3
Procedure
The same procedures used in Example 1 were repeated except for using 1.02 g of indole-4-carbaldehyde and (2-methyl-2-hepten-6-yl) methanesulfonate instead of the benzyl bromide used in Example 1 to give 1.36 g of 1-(2-methyl-2-hepten-6-yl)indole-4-carbaldehyde as a yellow oily substance. The yield thereof was found to be 76%.
Sources & evidence
- ORD record
- ord-004ee47338b3491ea0194fdef9d71d6a
- Source dataset
- uspto-grants-1998_09
- Patent number
- US05811439
Reaction notes
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