1-Chloro-3-methyl-2-butene → HCID 18973416, compound

HRID 2394430Notes

Reaction equation

HRID 2394430 reaction equation
[NH:1]1[C:9]2[CH:8]=[CH:7][CH:6]=[C:5]([CH:10]=[O:11])[C:4]=2[CH:3]=[CH:2]1.Cl[CH2:13][CH:14]=[C:15]([CH3:17])[CH3:16]>>[CH3:16][C:15]([CH3:17])=[CH:14][CH2:13][N:1]1[C:9]2[CH:8]=[CH:7][CH:6]=[C:5]([CH:10]=[O:11])[C:4]=2[CH:3]=[CH:2]1

Participants

3

Reactant 2

HCID 104291-Chloro-3-methyl-2-buteneHCID 333703Indole-4-carboxaldehyde

Product 1

HCID 18973416HCID 18973416, compound

Procedure

The same procedures used in Example 1 were repeated except for using 725 mg of indole-4-carbaldehyde and 1-chloro-3-methyl-2-butene instead of the benzyl bromide used in Example 1 to give 554 mg of 1-(3-methyl-2-butenyl)indole-4-carbaldehyde as an orange-colored oily substance. The yield thereof was found to be 52%.

Sources & evidence

ORD record
ord-457a823ebd6942dab35b267d5b24b9c5
Source dataset
uspto-grants-1998_09
Patent number
US05811439

Reaction notes

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