HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 4-Allyloxybenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4-(Prop-2-en-1-yloxy)benzoic acid | HCID 460690 | — |
| Catalyst | Pyridine | HCID 1049 | — |
| Product | 4-Allyloxybenzoyl chloride | HCID 11790137 | — |
Reaction Steps
The 4-(2-propenyloxy)benzoic acid, 5 g (0.028 mol), was refluxed with thionyl chloride (37 mL, 0.51 mol) and several drops of pyridine for 8 hours. The excess thionyl chloride was removed in vacuo leaving 4-(2-propenyloxy)benzoyl chloride as a yellow liquid at 25° C. This acid chloride was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05811504 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-eca76077e24e4d9686d7675b70148367 |
| Source note | uspto-grants-1998_09 |