HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 18974240, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Benzoic acid, 4-(5-hexenyloxy)- | HCID 11148720 | — |
| Catalyst | Pyridine | HCID 1049 | — |
| Product | HCID 18974240 | HCID 18974240 | — |
Reaction Steps
The 4-(5-hexenyloxy)benzoic acid 10 g (0.046 mol) was reflux with thionyl chloride (5.4 mL, 0.069 mol) and several drops of pyridine for 8 hours. The excess thionyl chloride was removed in vacuo leaving 4-(5-hexenyl-oxy)benzoyl chloride as a clear liquid at 25° C. This acid chloride was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05811504 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-2dbaf929f41346db97059ae934eabcf9 |
| Source note | uspto-grants-1998_09 |