Oxalyl chloride → HCID 10732797, compound

Participants

Reaction Conditions

Reaction Steps

2.8 ml (32.3 mmol) of oxalyl chloride were dissolved in 60 ml of CH2 Cl2. The solution was cooled at -10° C. and 6 g (19.0 mmol) of 7-methoxy-2-phenylquinoline-4-carboxylic acid were added portionwise. The reaction mixture was left overnight at room temperature and then evaporated to dryness to yield 7 g of the title compound, used without further purification.

Provenance & Evidence