HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 18630005, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 18630303 | HCID 18630303 | — |
| Product | HCID 18630005 | HCID 18630005 | — |
Reaction Steps
The compound of Example 50 (1.33 g, 5.0 mmol) and MeI (2.8 g, 20 mmol) were combined according to General Method B. The resulting reaction was partitioned between ethyl acetate and sat aq NaHCO3. The organic phase was washed with brine, dried (MgSO4), and concentrated to afford a quantitative yield of the title compound as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05811411 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-89b3f5fd77dd4dfb82397067a0b9912f |
| Source note | uspto-grants-1998_09 |