HCID 53917369, compound → 4,7-Methano-3aH-indene-3a-carboxylic acid, octahydro-, ethyl ester

Participants

Reaction Steps

The amount 1.3 g of 5%-Pd/C (with 50% moisture content) was added to 13.1 g of ethyl tricyclo[5.2.1.02,6 ]deca-8-ene-2-carboxylate obtained in the same procedures as in Example 1. The resultant mixture was stirred at 50° C. for 5 hours under hydrogen pressure of 5 kg/cm2. After the catalyst was removed by filtration, the filtrate was distilled to yield 12.3 g of ethyl tricyclo[5.2.1.02,6 ]decane-2-carboxylate. The yield was 93.0%.

Provenance & Evidence