Iodoethane → HCID 18974011, compound

Participants

Reaction Steps

To a mixture of methyl 4-[3-(2-benzyloxy-5-aminophenyl) propyl]benzoate (250 mg) in DMF (5 ml) was added potassium carbonate (0.2 g) and iodoethane (0.16 ml). The reaction was stirred for 18 hours, diluted with EtOAc, washed with water and brine, dried (MgSO4), filtered and evaporated. The residue was purified by flash chromatography to give the methyl 4-[3-(2-benzyloxy-5-(diethylamino) phenyl)propyl]benzoate as an oil (150 mg).

Provenance & Evidence