methyl 4-[2-(2-benzyloxyphenyl)-(E)-ethenyl]-2-methoxybenzoate → Methyl 4-[2-(2-benzyloxyphenyl)ethyl]-2-methoxybenzoate

HRID 2395020Notes

Reaction equation

HRID 2395020 reaction equation
C(OC1C=CC=CC=1CCC1C=CC(C(OC)=O)=C(O)C=1)C1C=CC=CC=1.[CH2:28]([O:35][C:36]1[CH:41]=[CH:40][CH:39]=[CH:38][C:37]=1/[CH:42]=[CH:43]/[C:44]1[CH:53]=[CH:52][C:47]([C:48]([O:50][CH3:51])=[O:49])=[C:46]([O:54][CH3:55])[CH:45]=1)[C:29]1[CH:34]=[CH:33][CH:32]=[CH:31][CH:30]=1>>[CH2:28]([O:35][C:36]1[CH:41]=[CH:40][CH:39]=[CH:38][C:37]=1[CH2:42][CH2:43][C:44]1[CH:53]=[CH:52][C:47]([C:48]([O:50][CH3:51])=[O:49])=[C:46]([O:54][CH3:55])[CH:45]=1)[C:29]1[CH:30]=[CH:31][CH:32]=[CH:33][CH:34]=1

Participants

3

Reactant 2

HCID 18973728methyl 4-[2-(2-benzyloxyphenyl)-(E)-ethenyl]-2-methoxybenzoateHCID 18973935Methyl 4-[2-(2-benzyloxyphenyl)ethyl]-2-hydroxybenzoate

Product 1

HCID 18974111Methyl 4-[2-(2-benzyloxyphenyl)ethyl]-2-methoxybenzoate

Procedure

Methyl 4-[2-(2-benzyloxyphenyl)ethyl]-2-methoxybenzoate was prepared from methyl 4-[2-(2-benzyloxyphenyl)ethyl]-2-hydroxybenzoate (prepared as described in Example 14) using the method described in Example 14 for the preparation of methyl 4-[2-(2-benzyloxyphenyl)-(E)-ethenyl]-2-methoxybenzoate.

Sources & evidence

ORD record
ord-17eac1422fc9451883483b21f1f0e88e
Source dataset
uspto-grants-1998_09
Patent number
US05811459

Reaction notes

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