HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropylethylamine → HCID 131720848, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | N-(9-Fluorenylmethoxycarbonyl)-O-tert-butylserine | HCID 2724633 | — |
| Reactant | O-(Benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate | HCID 2733207 | — |
| Reactant | HCID 131720849 | HCID 131720849 | — |
| Product | HCID 131720848 | HCID 131720848 | — |
Reaction Steps
250 mg of benzyl (6-aminomethyl-3,7-dimethoxy-10-hexyl-phenothiazin-4-yl)-acetate trifluoroacetate (1:1) were reacted with 153 mg of Fmoc-Ser(But)-OH, 141 mg of TBTU and 0.15 ml of DIPEA analogously to that described in Example 4.7.1. 20 mg of benzyl [6-((N-(9H-fluoren-9-ylmethoxycarbonyl)-O-tert.-butyl-L-seryl)-aminomethyl)-10-hexyl-3,7-dimethoxyphenothiazin-4-yl]-acetate were obtained; MS: 886.6 MH⊕.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05811389 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-5d08d8ec11b843b9996acb282ef36804 |
| Source note | uspto-grants-1998_09 |