Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Octylamine | HCID 8143 | — |
| Reactant | (2R,3S,4R,5R)-2,3,4,5,6-pentahydroxyhexanal | HCID 107526 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 11130076 | HCID 11130076 | — |
Reaction Steps
54 g of glucose (0.3 mol) are added to a solution of 40 g of octylamine (0.3 mol) in 50 ml of absolute methanol. The reaction mixture is heated to 65° C. for 20 min and then 50 ml of 95% hot ethanol are added. The N-octyl-β-D-glucopyranosylamine which precipitates on cooling (complete precipitation after 2 hours) is filtered off on a Buchner and then recrystallized from absolute ethand (1.5 1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05814407 |
|---|
| Source dataset | uspto-grants-1998_09 |
|---|
| ORD ID | ord-362e470a193645d9a420521e0d4c9e96 |
|---|
| Source note | uspto-grants-1998_09 |
|---|
