HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chloro-4-isothiocyanato-2-(trifluoromethyl)benzene → 1-[4-(2-Naphthylthio)phenyl]-3-(4-chloro-3-trifluoromethylphenyl)thiourea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chloro-4-isothiocyanato-2-(trifluoromethyl)benzene | HCID 520026 | — |
| Reactant | 2-(4-Aminophenylthio)naphthalene | HCID 18971645 | — |
| Product | 1-[4-(2-Naphthylthio)phenyl]-3-(4-chloro-3-trifluoromethylphenyl)thiourea | HCID 18971665 | 34.1% |
Reaction Steps
2-(4-Aminophenylthio)naphthalene (4.2 mmoles, 1.06 g) and 4-chloro-3-trifluoromethylphenylisothiocyanate (4.2 mmoles, 0.93 g) were reacted according to procedure A to yield of the title compound 0.7 g, 34%. Mass Spec (FD) 489. Calculated for C24H16ClF3 N2S2 : C, ; H, N, . Found: C, ; H, ; N, .
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05814646 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-e3aa56a3aa604fc08ad2126306180adc |
| Source note | uspto-grants-1998_09 |