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Ethyl Acetate → 2-(4-Aminophenylthio)naphthalene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl Acetate | HCID 8857 | — |
| 反応物 | 2-(4-Nitrophenylthio)naphthalene | HCID 18971685 | — |
| 触媒 | Palladium | HCID 23938 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | 2-(4-Aminophenylthio)naphthalene | HCID 18971645 | 47.6% |
反応手順
2-(4-nitrophenylthio)naphthalene (9.2 mmoles, 2.6 g) was dissolved in 50 ml ethanol and 20 ml ethyl acetate and hydrogenated for 16 hrs at room temperature over 1.0 g 5% Pd/C. The solution was filtered through celite and concentrated to yield 2-(4-aminophenylthio)naphthalene 1.1 g, 47%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05814646 |
| 出典データセット | uspto-grants-1998_09 |
| ORD ID | ord-867e6214f818442b8046c174f1b52166 |
| 出典メモ | uspto-grants-1998_09 |