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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2395449Generated: November 2, 2026

Methyl isothiocyanate → HCID 54517905, compound

https://huagongshe.com/reaction/2395449

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl isothiocyanateHCID 11167—
Reactant6-amino-3-(dimethyl)amino-1,2,3,4-tetrahydro-9H-carbazoleHCID 22611560—
SolventDichloromethaneHCID 6344—
ProductHCID 54517905HCID 5451790548%

Reaction Steps

To a solution of 10.0 mg (0.0437 mMol) 6-amino-3-(dimethyl)amino-1,2,3,4-tetrahydro-9H-carbazole in 3.0 mL dichloromethane were added 6.2 mg (0.0874 mMol) methyl isothiocyanate. The reaction was mixed for 48 hours and to it were then added 0.15 gm (0.0874 mMol) aminomethylated polystyrene and the reaction mixed for an additional 18 hours. The reaction mixture was then filtered and the volatiles evaporated to give 6.3 mg (48%) of the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05814653
Source datasetuspto-grants-1998_09
ORD IDord-796dff6d58734fcfb039157923635567
Source noteuspto-grants-1998_09