1-(4-Methylphenyl)propan-2-one → HCID 53928033, compound

HRID 2395716Notes

Reaction equation

HRID 2395716 reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][C:9](=[O:11])[CH3:10])=[CH:4][CH:3]=1.[OH:12][C:13]1[CH:14]=[C:15]([CH:18]=[C:19]([N+:22]([O-:24])=[O:23])[C:20]=1[OH:21])[CH:16]=O>>[OH:12][C:13]1[CH:14]=[C:15]([CH:16]=[C:8]([C:5]2[CH:6]=[CH:7][C:2]([CH3:1])=[CH:3][CH:4]=2)[C:9](=[O:11])[CH3:10])[CH:18]=[C:19]([N+:22]([O-:24])=[O:23])[C:20]=1[OH:21]

Participants

3

Reactant 2

HCID 1374281-(4-Methylphenyl)propan-2-oneHCID 57489573,4-Dihydroxy-5-nitrobenzaldehyde

Product 1

HCID 53928033HCID 53928033, compound

Procedure

The procedure described in Example 1 was repeated by using 0.81 g of 3-(4-methylphenyl)-2-propanone and 0.92 g of 3,4-dihydroxy-5-nitrobenzaldehyde. Yield 0.82 g, mp 189°-194° C.

Sources & evidence

ORD record
ord-d59a8de5b42f4e06b1670f2ef4668b2f
Source dataset
uspto-grants-1996_02
Patent number
US05489614

Reaction notes

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