HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2395728Generated: October 30, 2026
Trifluoroacetic acid → HCID 18990338, compound
https://huagongshe.com/reaction/2395728
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | 3,4-Heptanedione | HCID 83671 | — |
| Reactant | 5-(Hydroxymethyl)-3-nitrobenzene-1,2-diol | HCID 18990374 | — |
| Product | HCID 18990338 | HCID 18990338 | — |
Reaction Steps
A mixture containing 0.2 g of 3,4-dihydroxy-5-nitrobenzyl alcohol and 0.03 ml of trifluoroacetic acid in 2.5 ml of 3,4-heptanedione was heated for 20 h at 100° C. The solvent was evaporated in vacuo and the residue was recrystallized from 2-propanol. Yield 0.3 g, mp 126°-131° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05489614 |
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| Source dataset | uspto-grants-1996_02 |
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| ORD ID | ord-25e92bec5e6646baa2ab7a5488f9330f |
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| Source note | uspto-grants-1996_02 |
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