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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2395771Generated: November 3, 2026

2-Methylbenzaldehyde → HCID 54566374, compound

https://huagongshe.com/reaction/2395771

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-MethylbenzaldehydeHCID 10722—
ReactantMethyl 2-azidoacetateHCID 4020482—
ProductHCID 54566374HCID 54566374—

Reaction Steps

Following the general procedure of PREPARATION 61 and making non-critical variations but starting with o-tolualdehyde (5.0 g), methyl azidoacetate (19.2 g), the title compound is obtained, NMR (300 MHz, CDCl3) 7.96, 7.26-7.18, 7.13, 3.92 and 2.36 δ.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05489593
Source datasetuspto-grants-1996_02
ORD IDord-75e056adcc5e4b91bf87ba84c6b00dc5
Source noteuspto-grants-1996_02