Potassium thiocyanate → Ethyl 2,2-diethyl-4-thiocyanobutyrate

HRID 2395953Notes

Reaction equation

Cl[CH2:2][CH2:3][C:4]([CH2:12][CH3:13])([CH2:10][CH3:11])[C:5]([O:7][CH2:8][CH3:9])=[O:6].[S-:14][C:15]#[N:16].[K+]>>[CH2:10]([C:4]([CH2:12][CH3:13])([CH2:3][CH2:2][S:14][C:15]#[N:16])[C:5]([O:7][CH2:8][CH3:9])=[O:6])[CH3:11]

Participants

Reactant 2

HCID 516872Potassium thiocyanate

HCID 10512495Ethyl 4-chloro-2,2-diethylbutyrate

Product 1

HCID 10775774Ethyl 2,2-diethyl-4-thiocyanobutyrate

Procedure

Using ethyl 4-chloro-2,2-diethylbutyrate as obtained in Reference Example 8and potassium thiocyanate, the title compound was produced in the same manner as in Reference Example 11.

Sources & evidence

ORD record: ord-eb7618afc69346ba8ea2a13971b0db85
Source dataset: uspto-grants-1996_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05491145

Reaction notes

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