HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → 3-acetoxy-N-methyl-1-propanesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | 3-(Chlorosulfonyl)propyl acetate | HCID 10584211 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 3-acetoxy-N-methyl-1-propanesulfonamide | HCID 18988120 | — |
Reaction Steps
15 g of 3-acetoxy-1-propanesulfonylchloride was dissolved in 150 ml dichloromethane. To the mixture was added dropwise 11.6 g of methylamine (40% methanol solution) with stirring under ice coioling. The reaction mixture was stirred for 1.5 hours under ice cooling.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05491145 |
| Source dataset | uspto-grants-1996_02 |
| ORD ID | ord-398225994f194f91835c6e111caf7a50 |
| Source note | uspto-grants-1996_02 |