Hexylamine → 2-(2,6-Diisopropyl-phenylsulfamoyl)-N-hexyl-acetamide

HRID 2396097Notes

Reaction equation

[CH:1]([C:4]1[CH:9]=[CH:8][CH:7]=[C:6]([CH:10]([CH3:12])[CH3:11])[C:5]=1[NH:13][S:14]([CH2:17][C:18]([NH:20][C:21]1N=NN(CCCCCCCCCCCC)N=1)=[O:19])(=[O:16])=[O:15])([CH3:3])[CH3:2].[CH2:38](N)[CH2:39][CH2:40][CH2:41][CH2:42]C>>[CH:10]([C:6]1[CH:7]=[CH:8][CH:9]=[C:4]([CH:1]([CH3:2])[CH3:3])[C:5]=1[NH:13][S:14]([CH2:17][C:18]([NH:20][CH2:21][CH2:38][CH2:39][CH2:40][CH2:41][CH3:42])=[O:19])(=[O:16])=[O:15])([CH3:11])[CH3:12]

Participants

Reactant 2

HCID 8102Hexylamine

HCID 189886562-(2,6-Diisopropyl-phenylsulfamoyl)-N-(dodecyl-2-H-tetrazol-5-yl)-acetamide

Product 1

HCID 189886742-(2,6-Diisopropyl-phenylsulfamoyl)-N-hexyl-acetamide

Procedure

This compound was prepared in the same manner as for the title compound of Example 2, except that 2-DAT was replaced with N-hexylamine, mp 125°-127° C.

Sources & evidence

ORD record: ord-f91bc1a08eca4f5388d13031311d246d
Source dataset: uspto-grants-1996_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05491170

Reaction notes

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