1-Dodecanethiol → (2,6-Diisopropyl-phenylsulfamoyl)-thioacetic acid S-dodecyl ester

HRID 2396101Notes

Reaction equation

HRID 2396101 reaction equation
[CH:1]([C:4]1[CH:9]=[CH:8][CH:7]=[C:6]([CH:10]([CH3:12])[CH3:11])[C:5]=1[NH:13][S:14]([CH2:17][C:18](NC1N=NN(CCCCCCCCCCCC)N=1)=[O:19])(=[O:16])=[O:15])([CH3:3])[CH3:2].[CH3:38][CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH2:44][CH2:45][CH2:46][CH2:47][CH2:48][CH2:49][SH:50]>>[CH2:49]([S:50][C:18](=[O:19])[CH2:17][S:14](=[O:16])(=[O:15])[NH:13][C:5]1[C:4]([CH:1]([CH3:3])[CH3:2])=[CH:9][CH:8]=[CH:7][C:6]=1[CH:10]([CH3:11])[CH3:12])[CH2:48][CH2:47][CH2:46][CH2:45][CH2:44][CH2:43][CH2:42][CH2:41][CH2:40][CH2:39][CH3:38]

Participants

3

Reactant 2

HCID 81951-DodecanethiolHCID 189886562-(2,6-Diisopropyl-phenylsulfamoyl)-N-(dodecyl-2-H-tetrazol-5-yl)-acetamide

Product 1

HCID 15341058(2,6-Diisopropyl-phenylsulfamoyl)-thioacetic acid S-dodecyl ester

Procedure

This compound was prepared in the same manner as for the title compound of Example 2, except that 2-DAT was replaced with dodecylthiol, mp 58°-60° C.

Sources & evidence

ORD record
ord-d31bd723ecd041ef8b00f01885d64b1c
Source dataset
uspto-grants-1996_02
Patent number
US05491170

Reaction notes

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