HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 3,5-Bis(4-nitrophenoxy)benzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 3,5-Bis(4-nitrophenoxy)benzoic acid | HCID 16760376 | — |
| Product | 3,5-Bis(4-nitrophenoxy)benzoyl chloride | HCID 18988729 | — |
Reaction Steps
A mixture of 3,5-bis (4-nitrophenoxy) benzoic acid (51.9 g, 0.131 mol) and thionyl chloride (478 ml, 6.55 mol) are heated at reflux for 5 hours, with the excess thionyl chloride being removed by distillation. The residue is dried at 85° C. under vacuum overnight in the same reactor.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05491200 |
| Source dataset | uspto-grants-1996_02 |
| ORD ID | ord-6af97b4ef37c4fc7b612ac0d03298f08 |
| Source note | uspto-grants-1996_02 |