HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrabutylammonium Fluoride → HCID 15341205, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrabutylammonium Fluoride | HCID 2724141 | — |
| Reactant | HCID 15341204 | HCID 15341204 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 15341205 | HCID 15341205 | 96.3% |
Reaction Steps
A procedure similar to that described in Example 2, above, was followed, but using 700 mg of (4R,6R)-6-([1S,2S,6S,8S,8aR]-2-{1,2,6,7,8,8a-hexahydro-6-t-butyldimethylsilyloxy-8-[(2RS)-2-(2-isopropylphenoxy)butyryloxy]-2-methyl-1-naphthyl}ethyl)tetrahydro-4-t-butyldimethylsilyloxy-2H-pyran-2-one [prepared as describedin Example 7, above] and 14.0 ml of a 1.0 molar solution of tetrabutylammonium fluoride in tetrahydrofuran, to give 470 mg of the title compound as a colorless foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05491167 |
| Source dataset | uspto-grants-1996_02 |
| ORD ID | ord-4169390db22b445dae38fd6a8c13fe9f |
| Source note | uspto-grants-1996_02 |