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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2396231Generated: November 1, 2026

Tetrabutylammonium Fluoride → HCID 67730910, compound

https://huagongshe.com/reaction/2396231

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTetrabutylammonium FluorideHCID 2724141—
ReactantHCID 67730996HCID 67730996—
SolventTetrahydrofuranHCID 8028—
ProductHCID 67730910HCID 6773091090.7%

Reaction Steps

A procedure similar to that described in Example 2, above, was followed, but using 1.16 g of (4R,6R)-6-([1S,2S,6S,8S,8aR]-2-{1,2,6,7,8,8a-hexahydro-6-t-butyldimethylsilyloxy-8-[2-(4-trifluoromethylbenzyloxy)-2-methylpropionyloxy]-2-methyl-1-naphthyl}ethyl)tetrahydro-4-t-butyldimethylsilyloxy-2H-pyran-2-one [preparedas described in Example 145, above] and 20.4 ml of a 1.0 molar solution of tetrabutylammonium fluoride in tetrahydrofuran, to give 0.75 g of the title compound as a colorless foam.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05491167
Source datasetuspto-grants-1996_02
ORD IDord-68826500b5634964ae11ff0af6c24645
Source noteuspto-grants-1996_02