HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrabutylammonium Fluoride → HCID 54361726, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrabutylammonium Fluoride | HCID 2724141 | — |
| Reactant | HCID 53996491 | HCID 53996491 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 54361726 | HCID 54361726 | 79.2% |
Reaction Steps
A procedure similar to that described in Example 2, above, was followed, but using 548 mg of (4R,6R)-6-{(1S,2S,6S,8S,8aR)-2-[1,2,6,7,8,8a-hexahydro-6-t-butyldimethylsilyloxy-8-(2-ethyl-2-methoxybutyryloxy)-2-methyl-1-naphthyl]ethyl}tetrahydro-4-t-butyldimethylsiloxy-2H-pyran-2-one [prepared as described in Example 154, above] and 11.3 ml of a 1.0 molar solution of tetrabutylammonium fluoride in tetrahydrofuran, to give 288 mg of the title compound as a colorless foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05491167 |
| Source dataset | uspto-grants-1996_02 |
| ORD ID | ord-e9cb87794e5c435eb9196f3219424647 |
| Source note | uspto-grants-1996_02 |