HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrabutylammonium Fluoride → HCID 54529933, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrabutylammonium Fluoride | HCID 2724141 | — |
| Reactant | HCID 54300129 | HCID 54300129 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 54529933 | HCID 54529933 | 93.3% |
Reaction Steps
A procedure similar to that described in Example 2, above, was followed, but using 1.03 g of (4R,6R)-6-([1S,2S,6S,8S,8aR]-2-{1,2,6,7,8,8a-hexahydro-6-t-butyldimethylsilyloxy-8-[2-(4-fluorobenzyloxy)-2-methylpropionyloxy]-2-methyl-1-naphthyl}ethyl)tetrahydro-4-t-butyldimethylsilyloxy-2H-pyran-2-one [prepared as described in Example 166 , above] and 19.4 ml of a 1.0 molar solution of tetrabutylammonium fluoride in tetrahydrofuran, to give 666 mg of the title compound as a colorless foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05491167 |
| Source dataset | uspto-grants-1996_02 |
| ORD ID | ord-2d1d4bbd256e4c768c6261489ebb02d5 |
| Source note | uspto-grants-1996_02 |