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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2396243Generated: October 29, 2026

Tetrabutylammonium Fluoride → HCID 54529933, compound

https://huagongshe.com/reaction/2396243

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTetrabutylammonium FluorideHCID 2724141—
ReactantHCID 54300129HCID 54300129—
SolventTetrahydrofuranHCID 8028—
ProductHCID 54529933HCID 5452993393.3%

Reaction Steps

A procedure similar to that described in Example 2, above, was followed, but using 1.03 g of (4R,6R)-6-([1S,2S,6S,8S,8aR]-2-{1,2,6,7,8,8a-hexahydro-6-t-butyldimethylsilyloxy-8-[2-(4-fluorobenzyloxy)-2-methylpropionyloxy]-2-methyl-1-naphthyl}ethyl)tetrahydro-4-t-butyldimethylsilyloxy-2H-pyran-2-one [prepared as described in Example 166 , above] and 19.4 ml of a 1.0 molar solution of tetrabutylammonium fluoride in tetrahydrofuran, to give 666 mg of the title compound as a colorless foam.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05491167
Source datasetuspto-grants-1996_02
ORD IDord-2d1d4bbd256e4c768c6261489ebb02d5
Source noteuspto-grants-1996_02