Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2396245Generated: November 1, 2026

Tetrabutylammonium Fluoride → HCID 53864570, compound

https://huagongshe.com/reaction/2396245

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTetrabutylammonium FluorideHCID 2724141—
ReactantHCID 54208033HCID 54208033—
SolventTetrahydrofuranHCID 8028—
ProductHCID 53864570HCID 5386457091.5%

Reaction Steps

A procedure similar to that described in Example 2, above, was followed, but using 419 mg of (4R,6R)-6-{(1S,2S,6S,8S,8aR)-2-[1,2,6,7,8,8a-hexahydro-6-t-butyldimethylsilyloxy-8-(2-benzyloxy-2-methylpropionyloxy)-2-methyl-1-naphthyl]ethyl}tetrahydro-4-t-butyldimethylsilyloxy-2H-pyran-2-one [prepared as described in Example 169, above] and 8.1 ml of a 1.0 molar solution of tetrabutylammonium fluoride in tetrahydrofuran, to give 263 mg of the title compound as a colorless foam.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05491167
Source datasetuspto-grants-1996_02
ORD IDord-81e37424da7c463daab51f662e5a29f6
Source noteuspto-grants-1996_02