HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Adamantaneacetyl chloride → Sulfamic acid[adamantaneacetyl]-2,6-bis[1-methylethyl]phenyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Adamantaneacetyl chloride | HCID 2771882 | — |
| Reactant | Sulfamic acid[[2,6-bis(1-methylethyl)phenyl]-acetyl]-2,6-bis(1-methylethyl)phenyl ester | HCID 10226443 | — |
| Reactant | 2,6-Diisopropylphenylacetyl chloride | HCID 19362782 | — |
| Product | Sulfamic acid[adamantaneacetyl]-2,6-bis[1-methylethyl]phenyl ester | HCID 131719260 | — |
Reaction Steps
This compound was prepared in the same manner as for the title compound of Example 1, except that 2,6-diisopropylphenylacetyl chloride was replaced with adamantaneacetyl chloride; 1H NMR(CDCl3): 1.21 (d, 12H), 1.6-2.0 (m, 15H), 2.15 (s, 2H), 3.4 (m, 2H), 7.15-7.25 (m, 3H) ppm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05491172 |
| Source dataset | uspto-grants-1996_02 |
| ORD ID | ord-698a58ed5d0e4a1db473ad1447ac17f7 |
| Source note | uspto-grants-1996_02 |