2-Phenylpropionic acid → HCID 10157165, compound

HRID 2396277Notes

Reaction equation

HRID 2396277 reaction equation
CC([C:4]1[CH:9]=[CH:8][CH:7]=[C:6](C(C)C)[C:5]=1[CH2:13][C:14]([C:16]1[C:17]([CH:30]([CH3:32])[CH3:31])=[C:18]([O:25][S:26](=[O:29])(=[O:28])[NH2:27])[C:19]([CH:22]([CH3:24])[CH3:23])=[CH:20][CH:21]=1)=[O:15])C.[CH:33](C1C=CC=C(C(C)C)C=1CC(O)=O)(C)C.C1(C(C)C(O)=O)C=CC=CC=1>>[O:15]=[C:14]([C:16]1[C:17]([CH:30]([CH3:32])[CH3:31])=[C:18]([O:25][S:26](=[O:28])(=[O:29])[NH2:27])[C:19]([CH:22]([CH3:23])[CH3:24])=[CH:20][CH:21]=1)[CH:13]([C:5]1[CH:4]=[CH:9][CH:8]=[CH:7][CH:6]=1)[CH3:33]

Participants

4

Reactant 3

HCID 102962-Phenylpropionic acidHCID 10226443Sulfamic acid[[2,6-bis(1-methylethyl)phenyl]-acetyl]-2,6-bis(1-methylethyl)phenyl esterHCID 152779902-(2,6-Diisopropylphenyl)acetic acid

Product 1

HCID 10157165HCID 10157165, compound

Procedure

This compound was prepared in the same manner as for the title compound of Example 1, except that 2,6-diisopropylphenylacetic acid was replaced with 2-phenylpropionic acid, mp 142°-144° C.

Sources & evidence

ORD record
ord-f86a5be7b47049099498df504d1cf37b
Source dataset
uspto-grants-1996_02
Patent number
US05491172

Reaction notes

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